HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 2-(4-hydroxyphenoxy)acetate → 2-[4-[[4-[(2Z)-2-methoxyimino-2-phenylethoxy]phenyl]methoxy]phenoxy]acetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 2-(4-hydroxyphenoxy)acetate | HCID 13187337 | — |
| Reactant | (4-{[(2E)-2-(methoxyimino)-2-phenylethyl]oxy}phenyl)methanol | HCID 86695770 | — |
| Product | 2-[4-[[4-[(2Z)-2-methoxyimino-2-phenylethoxy]phenyl]methoxy]phenoxy]acetic acid | HCID 88583040 | 13.72% |
Reaction Steps
Compound 117 was synthesized from Intermediate 13 (0.22 g, 1.020 mmol) and ethyl (4-hydroxyphenoxy)acetate (0.20 g, 1.020 mmol) by following the procedure described in scheme 41 (0.060 g, yield: 13.72%); Purity: 97.98%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09278915B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-3efc166e44cc4582bf80489697961167 |
| Source note | uspto-grants-2016_03 |