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Methyl(3-bromopropyl)carbamate → Methyl (3-(3-iodo-6-methyl-1H-pyrazolo[3,4-b]pyridin-1-yl)propyl)carbamate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methyl(3-bromopropyl)carbamate | HCID 254236 | — |
| 反応物 | HCID 178422879 | HCID 178422879 | — |
| 生成物 | Methyl (3-(3-iodo-6-methyl-1H-pyrazolo[3,4-b]pyridin-1-yl)propyl)carbamate | HCID 68309959 | — |
反応手順
3-Iodo-6-methyl-1H-pyrazolo[3,4-b]pyridine and methyl (3-bromopropyl)carbamate were treated in the similar manner to Reference Example 102(1) to give methyl [3-(3-iodo-6-methyl-1H-pyrazolo[3,4-b]pyridin-1-yl)propyl]carbamate [REx(104-3)] as a colorless powder.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09278944B2 |
| 出典データセット | uspto-grants-2016_03 |
| ORD ID | ord-d0b1b78c72654bfdad207d88f651c119 |
| 出典メモ | uspto-grants-2016_03 |