HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → HCID 86729843, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | Hydrogen chloride-ethyl acetate | HCID 21866389 | — |
| Reactant | HCID 86729845 | HCID 86729845 | — |
| Product | HCID 86729843 | HCID 86729843 | — |
Reaction Steps
By a method similar to Example 1, Step C, 4N hydrochloric acid/ethyl acetate solution was added to N-{4-[trans-2-(benzylamino)cyclopropyl]phenyl}-3-(benzyloxy)benzamide obtained from N-[4-(trans-2-aminocyclopropyl)phenyl]-3-(benzyloxy)benzamide hydrochloride (109 mg) and benzaldehyde (29.3 μL), and the resulting solid was collected by filtration to give the title compound (96.1 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09278931B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-a9a668dcd73a4e7bac4c8dd75a3ff1d2 |
| Source note | uspto-grants-2016_03 |