HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 922562Generated: October 31, 2026
Potassium Carbonate → HCID 89654198, compound
https://huagongshe.com/reaction/922562
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-Bromo-5-hydroxypyridine | HCID 2762865 | — |
| Reactant | HCID 117696598 | HCID 117696598 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 89654198 | HCID 89654198 | — |
Reaction Steps
The mixture of 0.30 g (1.7 mmol) of 2-bromo-5-hydroxypyridine, 0.59 g (3.5 mmol) of 1-bromoethyl-2,2-difluorocyclopropane and 0.60 g (4.3 mmol) of K2CO3 in 10 ml ACN is stirred at 70° C. over night. The reaction mixture is filtered over alumina/activated carbon. The solvent is removed in vacuo.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US09278954B2 |
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| Source dataset | uspto-grants-2016_03 |
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| ORD ID | ord-d0f2de82ac274f11b144b6d892f93f6b |
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| Source note | uspto-grants-2016_03 |
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