HRID922629

反应详情

EQUATION

反应方程式

HRID 922629 的结构方程式

PROCEDURE

实验过程

4,5-Dichloroimidazole (1 mmol) will be dissolved into 1 mL of acetonitrile. Potassium hydroxide (0.061 g, 1.1 mmol) will be added and the mixture will be allowed to stir for 0.5 h. 2-bromoethylnaphthalene (1 mmol) will be added and the solution will be allowed to reflux overnight. The solution will be filtered hot to remove a white precipitate (presumed to be KBr) and the solution will be allowed to cool to room temperature. The volatiles will be removed en vacuo resulting in the product.

WORKUP

后处理

  1. temperatureto reflux overnight
  2. filtrationThe solution will be filtered hot
  3. customto remove a white precipitate (presumed to be KBr)
  4. customThe volatiles will be removed en vacuo
  5. customresulting in the product