HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetonitrile → HCID 70982804, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetonitrile | HCID 6342 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | 1-(2-Bromoethyl)naphthalene | HCID 139541 | — |
| Reactant | 4,5-Dichloroimidazole | HCID 140018 | — |
| Product | HCID 70982804 | HCID 70982804 | — |
Reaction Steps
4,5-Dichloroimidazole (1 mmol) will be dissolved into 1 mL of acetonitrile. Potassium hydroxide (0.061 g, 1.1 mmol) will be added and the mixture will be allowed to stir for 0.5 h. 2-bromoethylnaphthalene (1 mmol) will be added and the solution will be allowed to reflux overnight. The solution will be filtered hot to remove a white precipitate (presumed to be KBr) and the solution will be allowed to cool to room temperature. The volatiles will be removed en vacuo resulting in the product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09278951B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-9e40f8d775834cd593e56ee73978f895 |
| Source note | uspto-grants-2016_03 |