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HRID923114

反应详情

EQUATION

反应方程式

HRID 923114 的结构方程式

REACTANTS

反应物

2
结构：CC1CNCC(C)O1
HCID110862

2,6-Dimethyl morpholine

C6H13NO

结构：O=C(Nc1ccc(Cl)c(-c2ccccn2)c1)c1ccc(Cl)nc1
HCID58614810

6-Chloro-N-[4-chloro-3-(pyridin-2-yl)phenyl]pyridine-3-carboxamide

C17H11Cl2N3O

PRODUCTS

生成物

1
结构：CC1CN(c2ccc(C(=O)Nc3ccc(Cl)c(-c4ccccn4)c3)cn2)CC(C)O1
HCID58614663

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCCCO
溶剂HCID263

1-Butanol

C4H10O

PROCEDURE

实验过程

Procedure F was performed using 50 mg of 6-chloro-N-(4-chloro-3-(pyridin-2-yl)phenyl)nicotinamide and 90 μL of 2,6-dimethylmorpholine in 0.5 mL of BuOH. Purified by reverse phase HPLC to yield N-(4-chloro-3-(pyridin-2-yl)phenyl)-6-(2,6-dimethylmorpholino)nicotinamide. MS (Q1) 423.4 (M)+.

WORKUP

后处理

  1. customPurified by reverse phase HPLC