HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178473134, compound → HCID 178508560, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178473134 | HCID 178473134 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 178508560 | HCID 178508560 | 63% |
Reaction Steps
A solution of ethyl 2-(2-carbamimidoylhydrazinyl)-2-oxoacetic acid (2 g, 35.60 mmol) in water (100 ml) was stirred for 12 h at 100° C. The resulting mixture was concentrated under vacuum to give a residue, which was precipitated from water (10 ml) to afford 5-amino-1H-1,2,4-triazole-3-carboxylic acid as a white solid (1.1 g, 63%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09278973B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-66f730ea2d444e98a07c5f6d03710d8d |
| Source note | uspto-grants-2016_03 |