HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178513171, compound → 3-(3,4-dichlorophenyl)-1H-1,2,4-triazol-5-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178513171 | HCID 178513171 | — |
| Solvent | Water | HCID 962 | — |
| Product | 3-(3,4-dichlorophenyl)-1H-1,2,4-triazol-5-amine | HCID 178508294 | 89.3% |
Reaction Steps
A solution of 2-(3,4-dichlorobenzoyl)hydrazinecarboximidamide (9.5 g, 38.62 mmol) in water (150 ml) was stirred for 7 h at reflux. The solids were collected by filtration to afford 3-(3,4-dichlorophenyl)-1H-1,2,4-triazol-5-amine as an off-white solid (7.9 g, 89%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09278973B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-e9a07252ac00405191c3eb46ce821ad7 |
| Source note | uspto-grants-2016_03 |