HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methylbenzoic acid → 2-Methylbenzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methylbenzoic acid | HCID 8373 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Product | 2-Methylbenzoyl chloride | HCID 70276 | — |
Reaction Steps
A solution of 2-methylbenzoic acid (10 g, 1.00 equiv) in thionyl chloride (50 mL) was refluxed overnight at 80° C. in an oil bath. The reaction mixture was concentrated under vacuum to afford 2-methylbenzoyl chloride (crude) as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09278973B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-f8810eb9d488428ba8a3537d311d86c5 |
| Source note | uspto-grants-2016_03 |