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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 923354Generated: November 3, 2026

HCID 178424296, compound → HCID 178424211, compound

https://huagongshe.com/reaction/923354

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 178424296HCID 178424296—
SolventWaterHCID 962—
ProductHCID 178424211HCID 17842421166.2%

Reaction Steps

A solution of 2-(2-methylbenzoyl)hydrazinecarboximidamide (5 g) in water (40 mL) was stirred overnight at 100° C. The reaction mixture was diluted with H2O (20 mL) and the solid was collected by filtration and washed with water (20 mL) to afford 3-o-tolyl-1H-1,2,4-triazol-5-amine (3 g, 66% yield) as a white solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09278973B2
Source datasetuspto-grants-2016_03
ORD IDord-d368608fad6d4ec8b65788fc510db9ee
Source noteuspto-grants-2016_03