HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178424296, compound → HCID 178424211, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178424296 | HCID 178424296 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 178424211 | HCID 178424211 | 66.2% |
Reaction Steps
A solution of 2-(2-methylbenzoyl)hydrazinecarboximidamide (5 g) in water (40 mL) was stirred overnight at 100° C. The reaction mixture was diluted with H2O (20 mL) and the solid was collected by filtration and washed with water (20 mL) to afford 3-o-tolyl-1H-1,2,4-triazol-5-amine (3 g, 66% yield) as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09278973B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-d368608fad6d4ec8b65788fc510db9ee |
| Source note | uspto-grants-2016_03 |