Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 923426Generated: November 3, 2026

Trifluoroacetic acid → HCID 59540446, compound

https://huagongshe.com/reaction/923426

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
ReactantHCID 59540408HCID 59540408—
SolventDichloromethaneHCID 6344—
ProductHCID 59540446HCID 5954044677.1%

Reaction Steps

To a solution of product from example 122B (81 mg, 0.293 mmol) in CH2Cl2 (3 mL) was added 2,2,2-trifluoroacetic acid (1.5 mL, 0.293 mmol), and the resulting mixture was stirred at rt for 1 hr. The mixture was concentrated in vacuo to give the title compound (50 mg, 77%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09278922B2
Source datasetuspto-grants-2016_03
ORD IDord-aee99197c8d541ff8024caa0dc533eb8
Source noteuspto-grants-2016_03