HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 59540446, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 59540408 | HCID 59540408 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 59540446 | HCID 59540446 | 77.1% |
Reaction Steps
To a solution of product from example 122B (81 mg, 0.293 mmol) in CH2Cl2 (3 mL) was added 2,2,2-trifluoroacetic acid (1.5 mL, 0.293 mmol), and the resulting mixture was stirred at rt for 1 hr. The mixture was concentrated in vacuo to give the title compound (50 mg, 77%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09278922B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-aee99197c8d541ff8024caa0dc533eb8 |
| Source note | uspto-grants-2016_03 |