Hydrochloric Acid → HCID 59540152, compound

Participants

Reaction Steps

The product of example 128A (480 mg, 1.49 mmol) and NaOH (299 mg, 7.47 mmol) in MeOH (10 mL) was stirred at ambient temperature for 1 hour. The mixture had HCl (1M) added and was extracted with EtOAc. The organic was washed with brine, dried (MgSO4), filtered and concentrated to afford 310 mg (71%) of the title compound. MS (ESI) m/z 294 (M+H)+.

Provenance & Evidence