HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59540096, compound → HCID 59540360, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59540096 | HCID 59540096 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 59540360 | HCID 59540360 | 103% |
Reaction Steps
The product of example 128C (245 mg, 0.89 mmol) in trifluoroacetic acid (5 mL) was stirred at ambient temperature for 2 hours. The mixture was concentrated to afford 201 mg (100%) of the title compound. MS (ESI) m/z 276 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09278922B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-0020d13a381a40668d4b1850416a6ce0 |
| Source note | uspto-grants-2016_03 |