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HRID923708

反应详情

EQUATION

反应方程式

HRID 923708 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(C)OC(=O)N1CCC[C@H]1CO
HCID643448

N-Boc-L-prolinol

C10H19NO3

结构：CC(C)(C)OC(=O)N1C[C@@H](O[Si](C)(C)C(C)(C)C)C[C@H]1CO
HCID58303448

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)N1C[C@@H](O[Si](C)(C)C(C)(C)C)C[C@H]1C=O
HCID57754007

1,1-Dimethylethyl (2S,4S)-4-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-2-formyl-1-pyrrolidinecarboxylate

C16H31NO4Si

PROCEDURE

实验过程

With the exception that N-t-butoxycarbonyl-cis-4-(t-butyldimethylsilyl)oxy-L-prolinol, instead of N-t-butoxycarbonyl-L-prolinol, was used, the same procedure as in Preparation Example 1-1 was repeated to afford the title compound. 3.8 g (52%).

WORKUP

后处理

  1. customthe same procedure as in Preparation Example 1-1