HuagongsheHuagongshe Chemistry Print Report · For research reference only
(Pyrimidin-5-yl)boronic acid → HCID 89907684, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (Pyrimidin-5-yl)boronic acid | HCID 2795193 | — |
| Reactant | HCID 89907307 | HCID 89907307 | — |
| Product | HCID 89907684 | HCID 89907684 | — |
Reaction Steps
The title compound was prepared in an analogous fashion to that described in Example 133 using 6-(3,7-dioxa-9-azabicyclo[3.3.1]nonan-9-yl)-5-bromo-N-(4-(trifluoromethoxy)phenyl)nicotinamide (Stage 150.1) and pyrimidin-5-ylboronic acid to afford a solid. HPLC (Condition 4) tR=5.08 min, UPLC-MS (Condition 3) tR=1.00 min, m/z=488.2 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09278981B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-b92a4be0314e46258b54d6ae0616f2f9 |
| Source note | uspto-grants-2016_03 |