HRID924123

反应详情

EQUATION

反应方程式

HRID 924123 的结构方程式

PROCEDURE

实验过程

(3S,4S)-tert-Butyl 3-amino-4-hydroxypyrrolidine-1-carboxylate (0.3 g, 1.439 mmol) in 1.25 M HCl 1.25 M in EtOH (11.51 mL, 14.39 mmol) was stirred for 24 h at RT. The white suspension was evaporated to dryness under reduced pressure and the residue was suspended in MeOH (10 mL) and evaporated again to afford the title compound.

WORKUP

后处理

  1. customThe white suspension was evaporated to dryness under reduced pressure
  2. customevaporated again