HRID924136

反应详情

EQUATION

反应方程式

HRID 924136 的结构方程式

PROCEDURE

实验过程

The title compound was prepared in an analogous fashion to that described in Stage 169.2 using 4-(2-chloro-1,1,2,2-tetrafluoroethyl)aniline (Stage 278.3) and 5-bromo-6-chloronicotinic acid to afford a beige crystalline powder. HPLC (Condition 4) tR=6.77 min, UPLC-MS (Condition 3) tR=1.31 min, m/z=444.8 [M−H]−.

WORKUP

后处理

  1. customto afford a beige crystalline powder