HRID9248

反应详情

EQUATION

反应方程式

HRID 9248 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A solution of 2,4-dihydroxy-3-(2-propenyl)benzophenone (3 g) was reduced under ˜1 atm H2 in ethyl acetate (100 mL) over 10% Pd/C catalyst (0.3 grams) for 3 hours. The product was purified by crystallization from methanol/water. The product is obtained as small yellow plates.

WORKUP

后处理

  1. customThe product was purified by crystallization from methanol/water
  2. customThe product is obtained as small yellow plates