HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorodiisopropylphosphine → HCID 178425660, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorodiisopropylphosphine | HCID 538967 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Reactant | HCID 178425630 | HCID 178425630 | — |
| Product | HCID 178425660 | HCID 178425660 | — |
Reaction Steps
Procedure as described for NP Amidine I using the following amounts: 1.19 g of 4-methyl-N1-(2,6-dimethylphenyl)benzamidine (Amidine III, 5.0 mmol), 2.50 mL of 2.0 M butyllithium (5.0 mmol), 0.80 mL chlorodiisopropylphosphine (5.0 mmol). After filtration to remove lithium chloride and removal of solvent, a yellow oil was isolated (1.76 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09283555B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-7e05587c55fe4a859af7cc6655129a71 |
| Source note | uspto-grants-2016_03 |