HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorodiphenylphosphine → HCID 178438974, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorodiphenylphosphine | HCID 66180 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Reactant | HCID 178438972 | HCID 178438972 | — |
| Product | HCID 178438974 | HCID 178438974 | — |
Reaction Steps
Procedure as described for NP Amidine XVII using the following amounts: 1.26 g of N1-(2-n-propylphenyl)-4-methylbenzamidine (5.0 mmol), 2.50 mL of 2.0 M butyllithium (5.0 mmol), 0.90 mL of chlorodiphenylphosphine (5.0 mmol). 1.76 g (74%) of light yellow solid was collected.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09283555B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-9df29efe9ea3409e91330b90ada193b3 |
| Source note | uspto-grants-2016_03 |