HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 69045351, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 69044484 | HCID 69044484 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 69045351 | HCID 69045351 | — |
Reaction Steps
A solution of EXAMPLE 462A (1 g, 3.2 mmol) in 7N ammonia in methanol (5 ml) was heated at 70° C. overnight, and cooled to room temperature. The solid was collected by filtration, washed with methanol and dried to provide the title compound. MS (DCI/NH3) m/z 299 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09283222B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-b1edb49122c94178a0bfca2da6ce5092 |
| Source note | uspto-grants-2016_03 |