HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Aminothiophenol → HCID 68549937, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Aminothiophenol | HCID 8713 | — |
| Reactant | 4-Dimethylamino-2-nitrobenzaldehyde | HCID 291352 | — |
| Product | HCID 68549937 | HCID 68549937 | — |
Reaction Steps
The amine may be obtained, for example in analogy to methods described in DE-A-2333378. For example, the educts 2-aminothiophenol and 4-dimethylamino-2-nitrobenzaldehyde may be reacted to obtain (4-benzothiazol-2-yl-3-nitrophenyl)-dimethylamine, whose nitro group may be reduced to the amine in a conventional manner (e.g. using SnCl2/HCl), and the product is reacted with methane sulfochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09284278B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-12ecdd6a98fc462caa48707d068d46f0 |
| Source note | uspto-grants-2016_03 |