1,4-Dioxane hydrochloride → HCID 86725313, compound

Participants

Reaction Conditions

Reaction Steps

Into a glass vial, the product from step (a) (0.38 mmol) dissolved in 4N HCl/dioxane (2 ml) was added. The reaction mixture was stirred at 60° C. for 1 h. The mixture was cooled to room temperature and the solvent was evaporated in vacuo to give sub-titled compound as a brown solid that was used without further purification. MS: ESI (positive): 461 (M+1).

Provenance & Evidence