HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methoxyaniline → 1-(2-Amino-4-chloro-5-methoxyphenyl)ethanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methoxyaniline | HCID 10824 | — |
| Reactant | 3-Chloro-4-methoxyaniline | HCID 21441 | — |
| Product | 1-(2-Amino-4-chloro-5-methoxyphenyl)ethanone | HCID 66650482 | 50% |
Reaction Steps
1-(2-Amino-4-chloro-5-methoxy-phenyl)-ethanone 201g was synthesized from 3-chloro-4-methoxy-aniline 215g as a brown solid in 50% yield, according to the procedure as described for compound 215a. MS (ESI, EI+): m/z=200 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09284307B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-4ff61289c79e4b409326492a931081be |
| Source note | uspto-grants-2016_03 |