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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 926029Generated: October 30, 2026

Isopropylamine → HCID 68207821, compound

https://huagongshe.com/reaction/926029

Reaction equation

Participants

RoleNameHCIDCharge
ReactantIsopropylamineHCID 6363—
ReactantMethyl 3-(bromomethyl)benzoateHCID 517981—
SolventDimethylformamideHCID 6228—
ProductHCID 68207821HCID 6820782166.3%

Reaction Steps

A mixture of 2.00 g of methyl 3-(bromomethyl)benzoate, 1.55 g of isopropylamine, and 10 mL of DMF was stirred at room temperature overnight. The reaction mixture was concentrated under reduced pressure and the obtained residue was purified by silica gel column chromatography (chloroform-methanol) to obtain 1.20 g of methyl 3-[(isopropylamino)methyl]benzoate as a colorless solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09284295B2
Source datasetuspto-grants-2016_03
ORD IDord-2c702462257945128a21ec24bd175743
Source noteuspto-grants-2016_03