HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 66672546, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | (S)-tert-butyl (1-(methylsulfonyl)pyrrolidin-3-yl)carbamate | HCID 58959879 | — |
| Product | HCID 66672546 | HCID 66672546 | — |
Reaction Steps
4M HCl solution (in Dioxane) (2 mL) and (S)-tert-butyl (1-(methylsulfonyl)pyrrolidin-3-yl)carbamate (200 mg, 0.99 mmol) was stirred at 20-35° C. for 2 h. The solid precipitate thus obtained was filtered, washed with hexane and dried to afford 120 mg of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09289419B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-44e1e5ff0432417286e55ac956737ac5 |
| Source note | uspto-grants-2016_03 |