HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-Bis(benzyloxy)-6-chloropyridazine → HCID 86677034, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-Bis(benzyloxy)-6-chloropyridazine | HCID 12213474 | — |
| Reactant | HCID 86677027 | HCID 86677027 | — |
| Reactant | 4-Trifluoromethyl-1-phenylvinylboronic acid pinacol ester | HCID 86677032 | — |
| Product | HCID 86677034 | HCID 86677034 | 48% |
Reaction Steps
Prepared according to the method for 3,4-bis(benzyloxy)-6-(1-phenylethenyl)pyridazine (Intermediate 25) from 3,4-bis(benzyloxy)-6-chloropyridazine (Intermediate 1) and 4,4,5,5-tetramethyl-2-{1-[4-(trifluoromethyl)-phenyl]ethenyl}-1,3,2-dioxaborolane (Intermediate 66) in 48% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09290456B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-c8827ba687c04b40bc388f70523bc1cc |
| Source note | uspto-grants-2016_03 |