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HRID927158

反应详情

EQUATION

反应方程式

HRID 927158 的结构方程式

REACTANTS

反应物

2
结构：Clc1cccc(Cc2cc(OCc3ccccc3)c(OCc3ccccc3)nn2)c1
HCID71270271

未命名化合物

2 次

结构：O=c1[nH]nc(CCc2ccccc2)cc1O
HCID178518808

未命名化合物

PRODUCTS

生成物

1
结构：O=c1[nH]nc(Cc2cccc(Cl)c2)cc1O
HCID178518797

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCOC(C)=O
溶剂HCID8857

Ethyl acetate

C4H8O2

PROCEDURE

实验过程

Prepared in the same way as 4-hydroxy-6-(2-phenylethyl)pyridazin-3(2H)-one (Example 1) from 3,4-bis(benzyloxy)-6-[(3-chlorophenyl)methyl]pyridazine (Intermediate 48) except that the solvent used for the hydrogenation was ethyl acetate and the product was recrystallised from ethyl acetate.

WORKUP

后处理

  1. customthe product was recrystallised from ethyl acetate