HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13199823, compound → HCID 82125639, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13199823 | HCID 13199823 | — |
| Reactant | HCID 178418287 | HCID 178418287 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 82125639 | HCID 82125639 | — |
Reaction Steps
A suspension of 3A° molecular sieves (6.5 g) in CH2Cl2 (15 mL) was stirred at room temperature for 30 minutes and then PCC (pyridinium chlorochromate) (2 g) was added. To this PCC suspension, a solution of Compound H (1 g, 5.15 mmol) in dry CH2Cl2 (15 mL) was added dropwise and was stirred at room temperature for 3.5 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09290473B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-8bae8e74a6604d6ba370d9a9ed5b5a0b |
| Source note | uspto-grants-2016_03 |