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HRID927248

反应详情

EQUATION

反应方程式

HRID 927248 的结构方程式

REACTANTS

反应物

2
反应SMILES：CCS(=O)(=O)Cl
HCID11667

Ethanesulfonyl chloride

C2H5ClO2S

反应SMILES：COC(=O)CCCS(=O)(=O)N1C(=O)N(c2cccc(C(F)(F)F)c2)C2=C(C(=O)CC2)C1c1ccc(C#N)cc1
HCID90310908

未命名化合物

PRODUCTS

产物

1
反应SMILES：CCS(=O)(=O)N1C(=O)N(c2cccc(C(F)(F)F)c2)C2=C(C(=O)CC2)C1c1ccc(C#N)cc1
HCID90311581

未命名化合物

PROCEDURE

实验过程

The title compound is prepared in analogy to methyl 4-(4-(4-cyanophenyl)-2,5-dioxo-1-(3-(trifluoromethyl)phenyl)-6,7-dihydro-1H-cyclopenta[d]pyrimidin-3(2H,4H,5H)-yl-sulfonyl)butanoate (example 34), substituting 4-(chlorosulfonyl)butanoate with ethane-sulfonyl chloride. Yield: 11 mg; ESI mass spectrum [M+H]+=490; Retention time HPLC: 0.94 min (Z018_S04).

WORKUP

后处理

  1. custom0.94 min (Z018_S04)