HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 90310891, compound → HCID 90311549, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 90310891 | HCID 90310891 | — |
| Reactant | HCID 90310960 | HCID 90310960 | — |
| Product | HCID 90311549 | HCID 90311549 | — |
Reaction Steps
The title compound is prepared in analogy to 3-(methylsulfonyl)-4-(3-(methylsulfonyl)-2,5-dioxo-1-(2-(trifluoromethyl)pyridin-4-yl)-2,3,4,5,6,7-hexahydro-1H-cyclopenta[d]-pyrimidin-4-yl)benzonitrile (example 39), using 4-(2,5-dioxo-1-(2-(trifluoromethyl)pyridin-4-yl)-2,3,4, 5,6,7-hexahydro-1H-cyclopenta[d]pyrimidin-4-yl)benzonitrile (example 15.5, 60 mg, 0.15 mmol) as starting material. Yield: 30 mg; ESI mass spectrum [M+H]+=477; Retention time HPLC: 0.99 min (Z018_S04).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09290459B1 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-14ea446ed54b4a8cb111a07c8b9f1976 |
| Source note | uspto-grants-2016_03 |