HuagongsheHuagongshe Chemistry Print Report · For research reference only
Quinazolinedione → HCID 68388650, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Quinazolinedione | HCID 64048 | — |
| Reactant | Methyl 5-(bromomethyl)-2-fluorobenzoate | HCID 22645461 | — |
| Reactant | HCID 68388893 | HCID 68388893 | — |
| Product | HCID 68388650 | HCID 68388650 | — |
Reaction Steps
The title compound was prepared from quinazoline-2,4(1H,3H)-dione and methyl 5-(bromomethyl)-2-fluorobenzoate using a procedure similar to those described for the synthesis of compound of Example 1. 1H NMR (DMSO-d6): 11.75 (s, 1H), 8.00 (d, J=7.8 Hz, 1H), 7.84 (d, J=6.9 Hz, 1H), 7.67-7.55 (m, 2H), 7.32-7.21 (m, 3H), 5.32 (s, 2H), 3.81 (s, 3H). MS: m/z 329.1 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09290460B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-994807d3cd9e4e61b82aad8227f60930 |
| Source note | uspto-grants-2016_03 |