HuagongsheHuagongshe Chemistry Print Report · For research reference only
Solketal → HCID 68209381, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Solketal | HCID 7528 | — |
| Reactant | HCID 67465880 | HCID 67465880 | — |
| Solvent | 1,2-Dimethoxyethane | HCID 8071 | — |
| Product | HCID 68209381 | HCID 68209381 | — |
Reaction Steps
Potassium terbutylate (3.0 g, 26.7 mmoles) are added, in an inert atmosphere, to a solution of solketal (3.5 g, 26.7 mmoles) in 50.0 ml of 1,2-dimethoxyethane. After 20 minutes, 5.0 g of 2,7-dibromo-9,9-bis(3′-bromopropyl)fluorene (5.0 g, 8.9 mmoles) dissolved in 15.0 ml of 1,2-dimethoxyethane are added.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09290483B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-84c3bef1059a4d05a77f3e6de7bec0ad |
| Source note | uspto-grants-2016_03 |