Piconol → HCID 71087727, compound

HRID 927637Notes

Reaction equation

HRID 927637 reaction equation
[Br:1][C:2]1[CH:3]=[CH:4][C:5]([C:9]([OH:11])=[O:10])=[N:6][C:7]=1Cl.[N:12]1[CH:17]=[CH:16][CH:15]=[CH:14][C:13]=1[CH2:18][OH:19]>>[Br:1][C:2]1[CH:3]=[CH:4][C:5]([C:9]([OH:11])=[O:10])=[N:6][C:7]=1[O:19][CH2:18][C:13]1[CH:14]=[CH:15][CH:16]=[CH:17][N:12]=1

Participants

3

Reactant 2

HCID 11474PiconolHCID 446077145-Bromo-6-chloropicolinic acid

Product 1

HCID 71087727HCID 71087727, compound

Procedure

The title compound was synthesized in analogy to Example 9 d, using 5-bromo-6-chloro-pyridine-2-carboxylic acid and 2-pyridinemethanol (CAN 586-98-1) as starting materials, LC-MS (UV peak area/ESI) 100%, 308.9876 (M+H)+.

Workup

  1. customwas synthesized in analogy to Example 9 d

Sources & evidence

ORD record
ord-9a5fda4fd3fe442a85f67c45a7342879
Source dataset
uspto-grants-2016_03
Patent number
US09290451B2

Reaction notes

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