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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 928038Generated: October 30, 2026

HCID 70984611, compound → HCID 42579940, compound

https://huagongshe.com/reaction/928038

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 70984611HCID 70984611—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 42579940HCID 4257994090.9%

Reaction Steps

Palladium on carbon (10%, 0.3 g) was added to a solution of benzyl N—((S)-1-ethylpyrrolidin-3-ylmethyl)carbamate (Intermediate 170, 1.8 g) in methanol (20 mL) and the resultant mixture was stirred under an atmosphere of hydrogen for 24 hours. The mixture was filtered and the filtrate was evaporated to dryness to give ((S)-1-ethylpyrrolidin-3-yl)methylamine (0.8 g) as a colourless oil, which was used without further characterisation.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09290472B2
Source datasetuspto-grants-2016_03
ORD IDord-008ab6cc2d0440e796ea65c8ebe2bfac
Source noteuspto-grants-2016_03