Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Benzeneacetic acid, hydrazide | HCID 70301 | — |
| Reactant | Ethyl 2-ethoxy-2-iminoacetate | HCID 10920638 | — |
| Product | HCID 58081363 | HCID 58081363 | — |
Reaction Steps
Ethyl-2-ethoxy-2-iminoacetate (1.318 g, 9.08 mmol) and phenyl acetic acid hydrazide (1.364 g, 9.08 mmol) were mixed together in ethanol (20 ml) and stirred at 80° C. for 1 h. Ethanol was evaporated. The residue was dissolved in n-butanol (20 ml). The reaction mixture was stirred at 150° C. for 20 h, then solvents were evaporated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US09290485B2 |
|---|
| Source dataset | uspto-grants-2016_03 |
|---|
| ORD ID | ord-12d0f595110f482ea4f4751a12afcd85 |
|---|
| Source note | uspto-grants-2016_03 |
|---|
