4-Methoxybenzaldehyde → 5-(4-Methoxybenzyl)-2,2-dimethyl-1,3-dioxane-4,6-dione

HRID 928723Notes

Reaction equation

HRID 928723 reaction equation
[CH3:1][O:2][C:3]1[CH:10]=[CH:9][C:6]([CH:7]=O)=[CH:5][CH:4]=1.ClC1C=CC(C[CH:17]2[C:22](=[O:23])[O:21][C:20]([CH3:25])([CH3:24])[O:19][C:18]2=[O:26])=CC=1.BrC1C=C2C(=CC=1)N=C(Cl)C(CC1C=CC(Cl)=CC=1)=C2Cl>>[CH3:1][O:2][C:3]1[CH:10]=[CH:9][C:6]([CH2:7][CH:17]2[C:22](=[O:23])[O:21][C:20]([CH3:25])([CH3:24])[O:19][C:18]2=[O:26])=[CH:5][CH:4]=1

Participants

4

Reactant 3

HCID 312444-MethoxybenzaldehydeHCID 108801105-(4-Chlorobenzyl)-2,2-dimethyl-1,3-dioxane-4,6-dioneHCID 867155806-Bromo-2,4-dichloro-3-(4-chlorobenzyl)quinoline

Product 1

HCID 6655385-(4-Methoxybenzyl)-2,2-dimethyl-1,3-dioxane-4,6-dione

Procedure

The title compound was prepared using 4-methoxybenzaldehyde in place of 4-chlorobenzaldehyde using the procedure described for the preparation of 5-(4-chlorobenzyl)-2,2-dimethyl-1,3-dioxane-4,6-dione (Intermediate 3: step a).

Sources & evidence

ORD record
ord-4c4e947ae32a4ccaa6e3bd7c9d79bc5d
Source dataset
uspto-grants-2016_03
Patent number
US09290476B2

Reaction notes

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