HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Thiophenecarboxaldehyde → 1,3-Dioxane-4,6-dione, 2,2-dimethyl-5-(2-thienylmethyl)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Thiophenecarboxaldehyde | HCID 7364 | — |
| Reactant | 5-(4-Chlorobenzyl)-2,2-dimethyl-1,3-dioxane-4,6-dione | HCID 10880110 | — |
| Reactant | 6-Bromo-2,4-dichloro-3-(4-chlorobenzyl)quinoline | HCID 86715580 | — |
| Product | 1,3-Dioxane-4,6-dione, 2,2-dimethyl-5-(2-thienylmethyl)- | HCID 10955679 | — |
Reaction Steps
The title compound was prepared using thiophene-2-carbaldehyde in place of 4-chlorobenzaldehyde using the procedure described for the preparation of 5-(4-chlorobenzyl)-2,2-dimethyl-1,3-dioxane-4,6-dione (Intermediate 3: step a).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09290476B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-3639582d0c2e450aa1e2a8d649e58037 |
| Source note | uspto-grants-2016_03 |