HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Benzothiophene-2-carbaldehyde → 5-(Benzo[b]thiophen-2-ylmethyl)-2,2-dimethyl-1,3-dioxane-4,6-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Benzothiophene-2-carbaldehyde | HCID 736500 | — |
| Reactant | 5-(4-Chlorobenzyl)-2,2-dimethyl-1,3-dioxane-4,6-dione | HCID 10880110 | — |
| Reactant | 6-Bromo-2,4-dichloro-3-(4-chlorobenzyl)quinoline | HCID 86715580 | — |
| Product | 5-(Benzo[b]thiophen-2-ylmethyl)-2,2-dimethyl-1,3-dioxane-4,6-dione | HCID 86715589 | — |
Reaction Steps
The title compound was prepared using benzo[b]thiophene-2-carbaldehyde in place of 4-chlorobenzaldehyde using the procedure described for the preparation of 5-(4-chlorobenzyl)-2,2-dimethyl-1,3-dioxane-4,6-dione (Intermediate 3: step a).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09290476B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-1a54147a11a740f597ad00f10da1feba |
| Source note | uspto-grants-2016_03 |