Vanillin → Decylamine

HRID 928889Notes

Reaction equation

HRID 928889 reaction equation
O=[CH:2][C:3]1C=CC(O)=C(OC)[CH:4]=1.[CH:12]1[CH:17]=[C:16]([CH2:18]N)C=[C:14]([CH2:20][NH2:21])[CH:13]=1>>[CH3:2][CH2:3][CH2:4][CH2:18][CH2:16][CH2:17][CH2:12][CH2:13][CH2:14][CH2:20][NH2:21]

Participants

3

Reactant 2

HCID 1183VanillinHCID 151331,3-Benzenedimethanamine

Product 1

HCID 8916Decylamine

Procedure

according to the general preparation protocol for the reductive alkylation, 30.4 g of vanillin (=4-hydroxy-2-methoxybenzaldehyde) and 13.6 g of MXDA were reacted. There was obtained a clear, orange oil with a viscosity of 62,380 mPa·s at 60° C. and an amine content of 5.0 mmol N/g.

Workup

  1. customwere reacted
  2. customThere was obtained a clear, orange oil with a viscosity of 62,380 mPa·s at 60° C.

Sources & evidence

ORD record
ord-2c65695388c648a69f05b1fd96ff225b
Source dataset
uspto-grants-2016_03
Patent number
US09290609B2

Reaction notes

Loading…