HuagongsheHuagongshe Chemistry Print Report · For research reference only
Vanillin → Decylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Vanillin | HCID 1183 | — |
| Reactant | 1,3-Benzenedimethanamine | HCID 15133 | — |
| Product | Decylamine | HCID 8916 | — |
Reaction Steps
according to the general preparation protocol for the reductive alkylation, 30.4 g of vanillin (=4-hydroxy-2-methoxybenzaldehyde) and 13.6 g of MXDA were reacted. There was obtained a clear, orange oil with a viscosity of 62,380 mPa·s at 60° C. and an amine content of 5.0 mmol N/g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09290609B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-2c65695388c648a69f05b1fd96ff225b |
| Source note | uspto-grants-2016_03 |