Itaconic acid → 2-Hydroxyethyl Methacrylate

HRID 928891Notes

Reaction equation

HRID 928891 reaction equation
[CH2:1]([O:5]C(=O)C=C)[CH2:2]CC.[C:10]([OH:18])(=[O:17])[C:11]([CH2:13]C(O)=O)=[CH2:12].C(OS([O-])(=O)=O)CCCCCCCCCCC.[Na+]>>[CH3:13][C:11]([C:10]([O:18][CH2:2][CH2:1][OH:5])=[O:17])=[CH2:12]

Participants

4

Reactant 3

HCID 811Itaconic acidHCID 8846Butyl AcrylateHCID 3423265Sodium Lauryl Sulfate

Product 1

HCID 133602-Hydroxyethyl Methacrylate

Procedure

To the solution is added 19 g butylacrylate, 3 g itaconic acid and 1 g 30% sodium laurylsulfate solution. Polymerization is carried out as described before to obtain a stable latex with essentially no coagulum.

Workup

  1. customPolymerization
  2. customto obtain a stable latex with essentially no coagulum

Sources & evidence

ORD record
ord-b8f700816d25410099f798738a93bd02
Source dataset
uspto-grants-2016_03
Patent number
US09290639B2

Reaction notes

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