Tert-Butylamine → HCID 86718770, compound

HRID 929592Notes

Reaction equation

[Cl:1][C:2]1[CH:3]=[C:4]([C:9]2[CH:14]=[C:13]([CH:15]=O)[C:12]([OH:17])=[C:11]([C:18]3[CH:23]=[CH:22][C:21]([Cl:24])=[C:20]([Cl:25])[CH:19]=3)[CH:10]=2)[CH:5]=[CH:6][C:7]=1[Cl:8].[C:26]([NH2:30])([CH3:29])([CH3:28])[CH3:27]>>[ClH:1].[C:26]([NH:30][CH2:15][C:13]1[C:12]([OH:17])=[C:11]([C:18]2[CH:23]=[CH:22][C:21]([Cl:24])=[C:20]([Cl:25])[CH:19]=2)[CH:10]=[C:9]([C:4]2[CH:5]=[CH:6][C:7]([Cl:8])=[C:2]([Cl:1])[CH:3]=2)[CH:14]=1)([CH3:29])([CH3:28])[CH3:27]

Participants

Reactant 2

HCID 6385Tert-Butylamine

HCID 86718769HCID 86718769, compound

Product 1

HCID 86718770HCID 86718770, compound

Procedure

5′-((tert-Butylamino)methyl)-3,3″,4,4″-tetrachloro-[1,1′:3′,1″-terphenyl]-4′-ol hydrochloride was prepared as a white solid using the procedure described in Example 5 from 3,3″,4,4″-tetrachloro-4′-hydroxy-[1,1′:3′,1″-terphenyl]-5′-carbaldehyde and tert-butylamine.

Sources & evidence

ORD record: ord-569346112d7446348c212bd69383cd20
Source dataset: uspto-grants-2016_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US09296696B2

Reaction notes

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