HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-Dibromosalicylaldehyde → 3,3''-Dichloro-4'-hydroxy-4,4''-bis(trifluoromethyl)-[1,1':3',1''-terphenyl]-5'-carbaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-Dibromosalicylaldehyde | HCID 7024 | — |
| Reactant | 3-Chloro-4-(trifluoromethyl)benzeneboronic acid | HCID 3772958 | — |
| Reactant | 5'-((tert-Butylamino)methyl)-3,3''-dichloro-4,4''-bis(trifluoromethyl)-[1,1':3',1''-terphenyl]-4'-ol | HCID 86718773 | — |
| Product | 3,3''-Dichloro-4'-hydroxy-4,4''-bis(trifluoromethyl)-[1,1':3',1''-terphenyl]-5'-carbaldehyde | HCID 86718772 | — |
Reaction Steps
3,3″-Dichloro-4′-hydroxy-4,4″-bis(trifluoromethyl)-[1,1′:3′,1″-terphenyl]-5′-carbaldehyde was prepared using the procedure described in Intermediate 5 from 3,5-dibromosalicylaldehyde and 3-chloro-4-(trifluoromethyl)phenylboronic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09296696B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-5fe43679530b41eb98665fde661530ef |
| Source note | uspto-grants-2016_03 |