HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Chlorophenylhydrazine hydrochloride → HCID 89609975, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Chlorophenylhydrazine hydrochloride | HCID 75331 | — |
| Reactant | 5-(3-Chloro-5-fluorophenyl)-1-(pyridin-2-yl)-1H-pyrazole-3-carboxylic acid | HCID 89602575 | — |
| Reactant | HCID 131735140 | HCID 131735140 | — |
| Product | HCID 89609975 | HCID 89609975 | — |
Reaction Steps
240 mg (0.86 mmol) of the compound of Example 15A is reacted analogously to the synthesis of the compound of Example 20A with 230 mg (1.29 mmol) of 3-chlorophenylhydrazine hydrochloride. After hydrolysis, 21 mg (7% of theory) of the title compound is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09296720B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-dbf2f42353a34e0dab2f6cbfbde0a58d |
| Source note | uspto-grants-2016_03 |