HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Chloro-3-methoxy-pyridine-2-carboxylic acid → 4-Chloro-7-methoxypyrido(3,2-d)pyrimidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Chloro-3-methoxy-pyridine-2-carboxylic acid | HCID 84070468 | — |
| Reactant | HCID 178493687 | HCID 178493687 | — |
| Product | 4-Chloro-7-methoxypyrido(3,2-d)pyrimidine | HCID 86715901 | — |
Reaction Steps
Using an analogous reaction to that described for Intermediate 14, step 3, 7-methoxypyrido[3,2-d]pyrimidin-4(1H)-one was converted to the title compound. LC/MS (ESI+) m/z=196 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09296734B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-68cdb2d555de43d191cd428075329bde |
| Source note | uspto-grants-2016_03 |