HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 930523Generated: November 1, 2026
Thionyl Chloride → 1,5-Dimethyl-6-oxo-1,6-dihydro-pyridine-3-carbonyl chloride
https://huagongshe.com/reaction/930523
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 1,5-Dimethyl-6-oxo-1,6-dihydropyridine-3-carboxylic acid | HCID 21885925 | — |
| Product | 1,5-Dimethyl-6-oxo-1,6-dihydro-pyridine-3-carbonyl chloride | HCID 117889546 | 100% |
Reaction Steps
1,5-Dimethyl-6-oxo-1,6-dihydro-pyridine-3-carboxylic acid D1 (500.000 mg; 2.991 mmol) is suspended in thionyl chloride (2.000 ml; 27.536 mmol) and heated for 2 h at 60° C. The reaction mixture is concentrated under reduced pressure. And used in the next reaction without further purification (Yield: 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US09296748B2 |
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| Source dataset | uspto-grants-2016_03 |
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| ORD ID | ord-2629e3e720614e108bb7b741e31a794f |
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| Source note | uspto-grants-2016_03 |
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