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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 930655Generated: October 30, 2026

4-chloropyridine N-oxide → HCID 68658149, compound

https://huagongshe.com/reaction/930655

Reaction equation

Participants

RoleNameHCIDCharge
Reactant4-chloropyridine N-oxideHCID 70724—
Reactant(2,4-Dichlorophenyl)boronic acidHCID 2734659—
ProductHCID 68658149HCID 6865814950%

Reaction Steps

4-Chloropyridine-N-oxide (1.5 g, 12 mmol), 2,4-dichlorophenylboronic acid (5.4 g, 29 mmol) were reacted according to the procedure of Example 39 (step a) to provide the title compound (1.40 g, 50%) as a grey solid: 1H NMR (500 MHz, CD3OD) δ 8.26 (d, J=6.9 Hz, 2H), 7.53 (d, J=2.0 Hz, 1H), 7.37-7.35 (m, 3H), 7.29 (d, J=8.3 Hz, 1H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09296743B2
Source datasetuspto-grants-2016_03
ORD IDord-69901add863243558bc2b6ba5dfc7f40
Source noteuspto-grants-2016_03