HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-chloropyridine N-oxide → HCID 68658149, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-chloropyridine N-oxide | HCID 70724 | — |
| Reactant | (2,4-Dichlorophenyl)boronic acid | HCID 2734659 | — |
| Product | HCID 68658149 | HCID 68658149 | 50% |
Reaction Steps
4-Chloropyridine-N-oxide (1.5 g, 12 mmol), 2,4-dichlorophenylboronic acid (5.4 g, 29 mmol) were reacted according to the procedure of Example 39 (step a) to provide the title compound (1.40 g, 50%) as a grey solid: 1H NMR (500 MHz, CD3OD) δ 8.26 (d, J=6.9 Hz, 2H), 7.53 (d, J=2.0 Hz, 1H), 7.37-7.35 (m, 3H), 7.29 (d, J=8.3 Hz, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09296743B2 |
| Source dataset | uspto-grants-2016_03 |
| ORD ID | ord-69901add863243558bc2b6ba5dfc7f40 |
| Source note | uspto-grants-2016_03 |