2-Bromo-5-methylpyridine → HCID 57950421, compound

Participants

Role	Name	HCID	Charge
Reactant	2-Bromo-5-methylpyridine	HCID 564216	—
Reactant	2-Methoxy-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridine	HCID 44754862	—
Product	HCID 57950421	HCID 57950421	42.2%

Reaction Steps

2-Bromo-5-methylpyridine (2.93 g, 17.0 mmol) and 2-methoxy-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridine (3.34 g, 14.2 mmol) were reacted according to Example 31 (step a) to provide the title compound (1.2 g, 42%) as a brown solid: ESI MS m/z 201 [M+H]+.

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US09296743B2
Source dataset	uspto-grants-2016_03
ORD ID	ord-16d55bd2842647a2b7deeecb8384462a
Source note	uspto-grants-2016_03